无机标准物质
--- 美国SPEX CLP项目标液 ---
元素:5000mg/L: Al, Ca, Mg
2000mg/L: Fe
基体:5% HNO3
体积:500mL
编号:INT-A1
用途:Assurance 级,电感耦合等离子体发射光谱仪(ICP-AES)分析用元素标液。EPA合约实验室CLP项目标液。
证书:每份标液都附有一份内容详细的标准物质证书,证书报告标液中多至68种痕量杂质元素含量实际测量结果。
溯源:美国NIST SRM (Traceable by NIST SRM)
资质:美国实验室认可协会(A2LA)标准物质生产商认可证书(2495.01)和测试实验室认可证书(2495.02),遵循ISO 17034-2016, ISO 17025:2005, ISO 9001:2008规范。
生产商:美国SPEX公司
**应用参考 · INSTRUCTION**
每次测试开始和结束验证干扰和背景校正因子,另外每20个样品必需进行检测。标液INT-A1,稀释20倍,为溶液A,标液INT-A1稀释20倍再加标液INT-B3稀释100倍后混合,为溶液AB。溶液A和溶液AB用于最常见的干扰检测。一旦两种溶液配制好,需连续分析,从溶液A开始。
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (INT-A1) and Solution AB, a combination of interferents (INT-A1) and analytes (INT-B3). Solution A is prepared by diluting INT-A1 20-fold. Solution AB is prepared by diluting INT-A1 20-fold and INT-B3 100-fold; for example, 5 mL of INT-A1 and 1 mL of INT-B3 into a 100 mL volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.
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